5TK0 image
Deposition Date 2016-10-06
Release Date 2017-04-05
Last Version Date 2024-10-23
Entry Detail
PDB ID:
5TK0
Keywords:
Title:
Lysozyme structure collected with 3D printed polymer mounts
Biological Source:
Source Organism(s):
Gallus gallus (Taxon ID: 9031)
Method Details:
Experimental Method:
Resolution:
1.80 Å
R-Value Free:
0.29
R-Value Work:
0.20
R-Value Observed:
0.21
Space Group:
P 43 21 2
Macromolecular Entities
Structures with similar UniProt ID
Protein Blast
Polymer Type:polypeptide(L)
Molecule:Lysozyme C
Gene (Uniprot):LYZ
Chain IDs:A
Chain Length:128
Number of Molecules:1
Biological Source:Gallus gallus
Primary Citation
3D Printed Micrometer-Scale Polymer Mounts for Single Crystal Analysis.
Anal. Chem. 89 4405 4408 (2017)
PMID: 28319372 DOI: 10.1021/acs.analchem.7b00443

Abstact

3D printed micrometer-scale polymer mounts for single crystal analysis have been prepared by photopolymerization using digital light projection stereolithography (DLP-SLA), with a commercially available digital light projection stereolithography printer (US$4000) and 3DM-ABS resin (US$150 per liter). The polymer mounts were prepared in batches of 49 in 1 h 15 min, which allowed for rapid prototyping and testing of new crystal mounting designs, with a resin cost of 0.2¢ US per mount. The suitability of the 3D printed mounts for single crystal crystallography has been demonstrated through their use in Cu Kα X-ray diffraction experiments of Rochelle salt (sodium potassium tartrate), the protein lysozyme, and has been employed for routine crystallographic analysis of organic and inorganic materials.

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Primary Citation of related structures
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